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ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate

ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate

CAS: 59897-92-6

Molecular Formula: C10H15Cl3O2

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ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate - Names and Identifiers

Name ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate
Synonyms Ethyl 4,6,6-trichloro-3,3-dimethyl-5-hexenoate
ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate
ethyl 4,6,6-trichloro-3,3-dimethyl hexeno-5-ate
4,6,6-Trichloro-3,3-dimethyl-5-hexenoic acid ethyl ester
CAS 59897-92-6

ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate - Physico-chemical Properties

Molecular FormulaC10H15Cl3O2
Molar Mass273.58
Density1.3075 (rough estimate)
Boling Point383.71°C (rough estimate)
Refractive Index1.4521 (estimate)
Physical and Chemical PropertiesChemical quality This product is colorless or light yellow transparent liquid, B. p.91 ~ 92 ℃/53pa,n24D 1.4860, relative density 1.1 568, insoluble in water, soluble in organic solvents such as alcohol and ether.
UseUse 3, 3-dimethyl-4, 6, 6-trichloro hexene [5] Acid Ethyl Ester is an intermediate for the preparation of dichloro-pyrethric acid by means of the phase model-culalite process.

ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate - Upstream Downstream Industry

Raw MaterialsIsobutyric acid
1-Hexene
Triethyl orthoacetate
Downstream ProductsPermethric acid

ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate - Production method

its preparation method is to add 1,1, 1-trichloro-4-methyl-pentene [3] alcohol-[2] into a reaction kettle, then add triethyl orthoacetate and catalyst isobutyric acid, stir, heat, and introduce nitrogen, uniformly raise the temperature from 110 ℃ to 150 ℃ for about 12 hours, accompanied by distillate (mainly toluene, ethanol, ethyl acetate, etc.), the reaction was carried out at 150~155 ℃ for 7~8h, the end point was controlled by gas chromatography, the reaction was finished, cooled, and the former fraction was distilled at 0.08MPa pressure, and the rest was ethyl 3, 3-dimethyl -4,6, 6-trichlorohexene [5] acid.

Last Update:2024-04-10 22:29:15
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ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate
diquinoxalino[2,3-a:2',3'-c]phenazine
(4-BENZHYDRYLPIPERAZIN-1-YL)(5-(4-CHLOROPHENYL)-2-METHYL-7-(TRIFLUOROMETHYL)PYRAZOLO[1,5-A]PYRIMIDIN-3-YL)METHANONE
4-(trifluoromethoxy)phenacyl bromide
isooctyl isoundecyl phthalate
N-BOC-2-[2-(2-氨基-乙氧基)乙氧基]-乙胺
2-(BROMOMETHYL)PYRIDINE HYDROBROMIDE
N-[4-Oxo-2-(1H-tetrazol-5-yl)-4H-1-benzopyran-8-yl]-4-(4-phe...
O-Methyl (2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl)carbamothioate
1-环戊基-4-甲基苯
Raw Materials for ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate
Isobutyric acid
1-Hexene
Triethyl orthoacetate
Downstream Products for ethyl 4,6,6-trichloro-3,3-dimethyl-hex-5-enoate
Permethric acid
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